                   INSTRUMENT CONTROL PARAMETERS:    8890_GCMSD
                   --------------------------------------------

   D:\MassHunter\GCMS\1\methods\MA_HCrr.M
      Mon May 13 17:54:11 2024

Control Information
------- -----------

Sample Inlet             : GC
Injection Source         : GC ALS
Injection Location:  Front
Mass Spectrometer        : Enabled


 No Sample Prep method has been assigned to this method.


GC
GC Summary
Run Time                                     75 min
Post Run Time                                0 min

Oven
Temperature
Setpoint                                     On
(Initial)                                    60 °C
Hold Time                                    2 min
Post Run                                     60 °C
Program
#1 Rate                                      20 °C/min
#1 Value                                     120 °C
#1 Hold Time                                 0 min
#2 Rate                                      4 °C/min
#2 Value                                     290 °C
#2 Hold Time                                 27.5 min


Equilibration Time                           0.25 min
Max Temperature                              325 °C
Maximum Temperature Override                 Disabled
Slow Fan                                     Disabled

ALS
Front Injector
Syringe Size                                 10 μL
Injection Volume                             1 μL
Solvent A Washes (PreInj)                    9
Solvent A Washes (PostInj)                   9
Solvent A Volume                             4 μL
Solvent B Washes (PreInj)                    5
Solvent B Washes (PostInj)                   5
Solvent B Volume                             4 μL
Sample Washes                                1
Sample Wash Volume                           1 μL
Sample Pumps                                 6
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 μL/min
Solvent Wash Dispense Speed                  3000 μL/min
Sample Wash Draw Speed                       300 μL/min
Sample Wash Dispense Speed                   3000 μL/min
Injection Dispense Speed                     6000 μL/min
Viscosity Delay                              0 sec
Sample Depth                                 Disabled
Injection Type                               Standard
L1 Airgap                                    0 μL
Solvent Wash Mode                            A, B

Sample Overlap
Mode                                         Sample overlap is not enabled

ALS Errors                                   Pause for user interaction

Front MM Inlet He
Front MM Inlet He Temperature
Setpoint                                     On
(Initial)                                    300 °C

Mode                                         Splitless
Pressure                                     On    11.014 psi
Total Flow                                   On    24.257 mL/min
Septum Purge Flow                            On    3 mL/min
Septum Purge Flow Mode                       Standard
Pre-Run Flow Test                            Off
Gas Saver                                    On    20 mL/min after 5 min
Purge Flow to Split Vent                     20 mL/min at 3 min
Cryo                                         Off
Cryo Type                                    CO2
Liner                                        Agilent 5190-2295: 870 μL (Split, taper, wool, low pressure drop)

Column
Column #1
Flow
Setpoint                                     On
(Initial)                                    1.2574 mL/min
Post Run                                     1 mL/min

Column Information                           Agilent 19091S-433UI: 2274534H
Description                                  HP-5MS UI
Temperature Range                            -60 °C—325 °C (350 °C)
Dimensions                                   30 m x 250 μm x 0.25 μm (Uncalibrated)
Heater                                       Oven
Column lock                                  Unlocked
In                                           Front MM Inlet He
Out                                          MSD 
(Initial)                                    60 °C
Pressure                                     11.014 psi
Flow                                         1.2574 mL/min
Average Velocity                             41.067 cm/sec
Holdup Time                                  1.2175 min
Control Mode                                 Constant Flow

Column Outlet Pressure                       0 psi

Detector Evaluation
Perform Detector Evaluation Test             Off
Signal Selected                              No Signal Selected
Checkout Sample                              No Checkout Sample Selected

MSD Transfer Line
Temperature
Setpoint                                     On
(Initial)                                    280 °C


Signals
Signal #1: 
Description                                  None

Signal #2: 
Description                                  None

Signal #3: 
Description                                  None

Signal #4: 
Description                                  None

Signal #5: 
Description                                  None

Signal #6: 
Description                                  None

Signal #7: 
Description                                  None

Signal #8: 
Description                                  None




MS Information
-- -----------


General Information
------- -----------


Acquisition Mode         : SIM
Solvent Delay (minutes)  : 5
Tune file                : D:\MassHunter\GCMS\1\5977\etune.u
EM Setting mode Gain     : 1.000000

Number of SIM Groups     : 1
Run Time (if MS only)    : 10 minutes 

[SIM Parameters]
Group 1               Group ID                  : 1
Resolution                : 1
Group Start Time          : 5
Number of Ions            : 22
Ions
Dwell In Group            :(  Mass,  Dwell) (  Mass,  Dwell)  (  Mass,  Dwell) 
                           (  85.10,40  )  (  113.10,40  )  (  125.10,40  ) 
                           (  142.20,40  )  (  177.20,40  )  (  178.20,40  ) 
                           (  183.00,40  )  (  184.20,40  )  (  189.20,40  ) 
                           (  191.20,65  )  (  192.20,40  )  (  198.20,40  ) 
                           (  205.20,40  )  (  215.20,40  )  (  217.20,40  ) 
                           (  218.20,40  )  (  221.20,40  )  (  231.30,40  ) 
                           (  245.30,40  )  (  253.30,40  )  (  257.30,40  ) 
                           (  259.30,40  ) 


[MSZones]

MS Source                   : 230 C   maximum 250 C
MS Quad                     : 150 C   maximum 200 C

Timed Events
----- ------
Number Events= 0



                     END OF MS ACQUISITION PARAMETERS


                        TUNE PARAMETERS for SN: US2219M015
                        ---------------------------------

 Trace Ion Detection is OFF.

    34.593   :   EMISSION     
    70.007   :   ENERGY       
     0.503   :   REPELLER     
    89.822   :   IONFOCUS     
    20.181   :   ENTRANCE_LENS
  1913.020   :   EMVOLTS      
                              2145.6  : Actual EMV 
                               1.00   : GAIN FACTOR 
  3429.000   :   AMUGAIN      
   131.188   :   AMUOFFSET    
     1.000   :   FILAMENT     
     0.000   :   DCPOLARITY   
    10.116   :   ENTLENSOFFSET
     8.502   :   Ion_Body     
    -0.098   :   EXTLENS      
   449.000   :  MASSGAIN        
   -23.000   :  MASSOFFSET      

                        END OF TUNE PARAMETERS
                        ----------------------



                       END OF INSTRUMENT CONTROL PARAMETERS
                       ------------------------------------
