

                     INSTRUMENT CONTROL PARAMETERS:    Instrument #1
                     -----------------------------------------------

   C:\MSDCHEM\1\METHODS\PTV METHODS\4THYEARPROJECTHCPTV.M

Control Information
------- -----------
       Sample Inlet : GC
   Injection Source : GC/ALS
 Injection Location : ALS
             Use MS : Yes

=============================================================================
                                6890 GC METHOD
=============================================================================

OVEN
   Initial temp:  60 'C (On)               Maximum temp:  325 'C
   Initial time:  2.00 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time
      1 20.00      120        0.00
      2  4.00      290       27.50
      3   0.0(Off)
   Post temp:  0 'C
   Post time:  0.00 min
   Run time:  75.00 min

FRONT INLET (HP PTV)                    BACK INLET (SPLIT/SPLITLESS)
   Mode:  Splitless                        Mode:  Split
   Initial temp:  300 'C (On)              Initial temp:  50 'C (Off)
   Initial time:  75.00 min                Pressure:  0.00 psi (Off)
   Ramps:                                  Total flow:  45.0 mL/min
      #  Rate  Final temp  Final time      Gas saver:  Off
      1   0.0(Off)                         Gas type:  Helium
   Cryo:  Off
   Cryo use temp:  25 'C
   Cryo Timeout:  30.00 min (On)
   Cryo Fault:  On
   Pressure:  9.98 psi (On)
   Purge flow:  5.0 mL/min
   Purge time:  2.00 min
   Total flow:  8.8 mL/min
   Gas saver:  On
   Saver flow:  15.0 mL/min
   Saver time:  5.00 min
   Gas type:  Helium

COLUMN 1                                COLUMN 2
   Capillary Column                        Capillary Column
   Model Number:  Greyhoun 10-200349       Model Number:  Agilent 122-1032
   GC-5                                    DB-1
   Max temperature:  325 'C                Max temperature:  325 'C
   Nominal length:  30.0 m                 Nominal length:  30.0 m
   Nominal diameter:  250.00 um            Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um        Nominal film thickness:  0.25 um
   Mode:  constant flow                    Inlet:  (unspecified)
   Initial flow:  1.2 mL/min               Outlet:  MSD
   Nominal init pressure:  9.99 psi
   Average velocity:  39 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum

FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)

SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0

COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)

THERMAL AUX 2                           AUX PRESSURE 3
   Use:  MSD Transfer Line Heater          Description:  Flow splitter
   Description:                            Gas Type:  Helium
   Initial temp:  280 'C (On)              Initial pressure:  0.00 psi (Off)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)

AUX PRESSURE 4                          AUX PRESSURE 5
   Description:                            Description:
   Gas Type:  Helium                       Gas Type:  Helium
   Initial pressure:  0.00 psi (Off)       Initial pressure:  0.00 psi (Off)

                                        POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time       Specifier                     Parameter & Setpoint


                               GC Injector


     Front Injector:
        Sample Washes                 2
        Sample Pumps                  6
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       3
        PreInj Solvent B Washes       3
        PostInj Solvent A Washes      4
        PostInj Solvent B Washes      4
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes

     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB006
 Column 2 Inventory Number : AB002

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : SIM


MS Information
-- -----------

Solvent Delay            : 6.00 min

EM Absolute              : False
EM Offset                : 0
Resulting EM Voltage     : 1623.5

[Sim Parameters]

GROUP 1
Group ID                 : 1
Resolution               : High
Plot 1 Ion               : 85.10
Plot 2 Ion               : 85.1
Ions/Dwell In Group      (  Mass,  Dwell) (  Mass,  Dwell) (  Mass,  Dwell) 
                         ( 83.10,    100) ( 85.10,     40) (113.10,    100) 
                         (125.10,    100) (133.20,    100) (134.20,    100) 
                         (142.20,    100) (156.20,    100) (166.20,    100) 
                         (177.20,    100) (178.20,     40) (180.20,    100) 
                         (183.20,    100) (184.20,    100) (189.20,    100) 
                         (191.20,     40) (192.20,     40) (198.20,    100) 
                         (202.20,    100) (205.20,    100) (215.20,    100) 
                         (216.20,    100) (217.20,     40) (218.20,     40) 
                         (228.20,    100) (231.30,     40) (242.30,    100) 
                         (245.30,    100) (252.30,    100) (253.30,     40) 
                         (256.30,    100) (257.30,    100) (259.30,    100) 
                         (267.30,    100) (276.30,    100) (352.40,    100) 
                         (412.40,     40) (422.40,    100) 

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C
Timed Events
----- ------

[Timed MS Detector Entries]

Time (min)          State (MS on/off)
6.00                     On
75.00                    Off


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN:  
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      34.814
 IONFOCUS    :      90.157
 ENTRANCE_LE :      25.500
 EMVOLTS     :    1623.529
 AMUGAIN     :    2054.000
 AMUOFFSET   :     122.250
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      17.820
 MASSGAIN    :    -387.000   
 MASSOFFSET  :     -43.000   


                           END OF TUNE PARAMETERS
                      ------------------------------------



                           END OF INSTRUMENT CONTROL PARAMETERS
                           ------------------------------------

