

                         INSTRUMENT CONTROL PARAMETERS:    Instrument #1
                         -----------------------------------------------

   C:\MSDCHEM\1\METHODS\PTV METHODS\4thyrprojectSIMAROMPTV.M

Control Information
------- -----------
       Sample Inlet : GC
   Injection Source : GC/ALS
 Injection Location : ALS
             Use MS : Yes

=============================================================================
                                6890 GC METHOD
=============================================================================

OVEN
   Initial temp:  60 'C (On)               Maximum temp:  325 'C
   Initial time:  2.00 min                 Equilibration time:  0.50 min
   Ramps:
      #  Rate  Final temp  Final time
      1 20.00      120        0.00
      2  4.00      290       17.50
      3   0.0(Off)
   Post temp:  0 'C
   Post time:  0.00 min
   Run time:  65.00 min

FRONT INLET (HP PTV)                    BACK INLET (SPLIT/SPLITLESS)
   Mode:  Splitless                        Mode:  Split
   Initial temp:  300 'C (On)              Initial temp:  50 'C (Off)
   Initial time:  0.00 min                 Pressure:  0.00 psi (Off)
   Ramps:                                  Total flow:  45.0 mL/min
      #  Rate  Final temp  Final time      Gas saver:  Off
      1   0.0(Off)                         Gas type:  Helium
   Cryo:  Off
   Cryo use temp:  25 'C
   Cryo Timeout:  30.00 min (On)
   Cryo Fault:  On
   Pressure:  11.72 psi (On)
   Purge flow:  10.0 mL/min
   Purge time:  65.00 min
   Total flow:  14.0 mL/min
   Gas saver:  On
   Saver flow:  20.0 mL/min
   Saver time:  65.00 min
   Gas type:  Helium

COLUMN 1                                COLUMN 2
   Capillary Column                        Capillary Column
   Model Number:  Greyhoun 10-200349       Model Number:  Agilent 122-1032
   GC-5                                    DB-1
   Max temperature:  325 'C                Max temperature:  325 'C
   Nominal length:  30.0 m                 Nominal length:  30.0 m
   Nominal diameter:  250.00 um            Nominal diameter:  250.00 um
   Nominal film thickness:  0.25 um        Nominal film thickness:  0.25 um
   Mode:  constant pressure                Inlet:  (unspecified)
   Pressure:  11.72 psi                    Outlet:  MSD
   Nominal initial flow:  1.3 mL/min
   Average velocity:  42 cm/sec
   Inlet:  Front Inlet
   Outlet:  MSD
   Outlet pressure:  vacuum

FRONT DETECTOR (NO DET)                 BACK DETECTOR (NO DET)

SIGNAL 1                                SIGNAL 2
   Data rate:  20 Hz                       Data rate:  20 Hz
   Type:  test plot                        Type:  test plot
   Save Data:  Off                         Save Data:  Off
   Zero:  0.0 (Off)                        Zero:  0.0 (Off)
   Range:  0                               Range:  0
   Fast Peaks:  Off                        Fast Peaks:  Off
   Attenuation:  0                         Attenuation:  0

COLUMN COMP 1                           COLUMN COMP 2
   (No Detectors Installed)                (No Detectors Installed)

THERMAL AUX 2                           AUX PRESSURE 3
   Use:  MSD Transfer Line Heater          Description:  Flow splitter
   Description:                            Gas Type:  Helium
   Initial temp:  280 'C (On)              Initial pressure:  0.00 psi (Off)
   Initial time:  0.00 min
      #  Rate  Final temp  Final time
      1   0.0(Off)

AUX PRESSURE 4                          AUX PRESSURE 5
   Description:                            Description:
   Gas Type:  Helium                       Gas Type:  Helium
   Initial pressure:  0.00 psi (Off)       Initial pressure:  0.00 psi (Off)

                                        POST RUN
                                           Post Time: 0.00 min

TIME TABLE
   Time       Specifier                     Parameter & Setpoint


                               GC Injector


     Front Injector:
        Sample Washes                 2
        Sample Pumps                  6
        Injection Volume           1.00 microliters
        Syringe Size               10.0 microliters
        PreInj Solvent A Washes       3
        PreInj Solvent B Washes       3
        PostInj Solvent A Washes      4
        PostInj Solvent B Washes      0
        Viscosity Delay               0 seconds
        Plunger Speed              Fast
        PreInjection Dwell         0.00 minutes
        PostInjection Dwell        0.00 minutes

     Back Injector:
No parameters specified

 Column 1 Inventory Number : AB006
 Column 2 Inventory Number : AB002

                                MS ACQUISITION PARAMETERS


General Information
------- -----------

Tune File                : atune.u
Acquistion Mode          : SIM


MS Information
-- -----------

Solvent Delay            : 5.00 min

EM Absolute              : True
Resulting EM Voltage     : 1047.1

[Sim Parameters]

GROUP 1
Group ID                 : 1
Resolution               : Low
Plot 1 Ion               : 156.20
Plot 2 Ion               : 178.2
Ions/Dwell In Group      (  Mass,  Dwell) (  Mass,  Dwell) (  Mass,  Dwell) 
                         (142.20,    100) (156.20,    100) (166.20,    100) 
                         (178.20,    100) (180.20,    100) (184.20,    100) 
                         (192.20,    100) (198.20,    100) (202.20,    100) 
                         (216.20,    100) (217.20,    100) (228.30,    100) 
                         (231.30,    100) (242.30,    100) (245.30,    100) 
                         (252.30,    100) (253.30,    100) (256.30,    100) 
                         (267.30,    100) (276.30,    100) 

[MSZones]

MS Quad                  : 150 C   maximum 200 C
MS Source                : 230 C   maximum 250 C
Timed Events
----- ------

[Timed MS Detector Entries]

Time (min)          State (MS on/off)
5.00                     On
85.00                    Off


                             END OF MS ACQUISITION PARAMETERS


                              TUNE PARAMETERS for SN:  
                        -----------------------------

 EMISSION    :      34.610
 ENERGY      :      69.922
 REPELLER    :      34.814
 IONFOCUS    :      90.157
 ENTRANCE_LE :      28.500
 EMVOLTS     :    1670.588
 AMUGAIN     :    2062.000
 AMUOFFSET   :     123.125
 FILAMENT    :       1.000
 DCPOLARITY  :       0.000
 ENTLENSOFFS :      17.569
 MASSGAIN    :    -400.000   
 MASSOFFSET  :     -42.000   


                           END OF TUNE PARAMETERS
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                              END OF INSTRUMENT CONTROL PARAMETERS
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